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Description:
Jacketed Glass Reactor (Double layer Glass Reactor) When the material is heated and reacted, the evaporation efficiency can be improved under vacuum condition (need to connect the vacuum device), and the solvent vapor can be cooled into liquid when it is cooled through the glass condensation coil (need to connect the cooling device), which can be refluxed back to kettle, and can also be recovered through the valve under the reflux elbow. When the reaction is finished, the material can be discharged from the side outlet at the bottom of the kettle.Reaction vessels also operate under vacuum making them ideal for any atmospheric sensitive applications. They can be made out of glass and range in volume from 1L to 200L.
Working principle:
This Jacketed Glass Reactor (Double layer Glass Reactor) has electric constant speed stirring system, condensation and dropping system. The interlayer of kettle body needs to be connected with heating or cooling circulation equipment. When the material is stirred, the circulating hot solution or cooling liquid is injected through the interlayer to make the materials in the kettle are heated or cooled at a constant temperature. When the material is heated and reacted, the evaporation efficiency can be improved under vacuum conditions (a vacuum device need to be connected). The solvent vapor is cooled into liquid when passing through the glass condensing coil (a cooling device need to be connected), which can be refluxed into the kettle. It can also be recycled through the lower valve of the dean-stark. When the reaction is completed, the material can be discharged from the side outlet at the bottom of the kettle.
This series of products need to be equipped with a vacuum device, a high-temperature or low-temperature circulation device to form system devices.
Feature:
1. The parts in contact with the material are all made of high borosilicate glass (expansion coefficient 3.3) and PTFE materials, which have stable performance and are not easy to react with the materials.
2. Using aluminum alloy + stainless steel material as base plate body
3. Glass + PTFE discharging valve, side material discharge without effusion.
4.Electronic stepless speed regulation, fine-adjustment by knob, digital display of speed
5. The stirring system adopts double bearings and double frame oil seal.
6. Vacuum pressure gauge displays real-time vacuum by pointer.
7. Crescent type stirring paddle, 304 stainless steel + PTFE stirring blade; the material of the stirring rod is 304 stainless steel, and it is wrapped in PTFE tube outside.
8. Fuse safety protection



Model |
GR-1 |
|
Kettle volume |
1L, inner diameter 120mm, outer diameter 150mm, inner length 160mm |
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Jacketed volume |
about 200ml |
|
Voltage/frequency |
220V/50HZ |
|
Stirring power |
40W |
|
Stirring speed |
0-1100r/min |
|
Temperature range vessel can bear |
-80 ℃ to 250 ℃ |
|
Temperature accuracy |
±1℃ |
|
Vacuum degree |
0.098Mpa |
|
Cover diameter |
Φ150mm |
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5port of the cover |
Stirring port |
Φ50mm flange port |
Condenser port |
24# standard port |
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Constant pressure funnel port |
24# standard port |
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Relief port |
19# standard port |
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Temperature measure port |
19# standard port |
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Stirring paddle |
Φ10*450H(mm), leafing 80mm |
|
Condenser size |
Φ40*350H(mm), upper with 24# standard port, down with 24# standard plug |
|
Constant pressure funnel |
250ml, upper with 24# standard port matched with glass plug, down with 24# standard plug |
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Relief valve |
19# standard plug valve, vent nozzle(Pagoda joint),outer diameter 10mm |
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Temperature measuring port |
19# standard plug, glass temperature measuring port |
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In and out circulation port of the sandwich |
Φ35 flange port matched with ring flange, adapter pagoda connector ,outer diameter 15mm |
|
Baiting port |
Screw port matched with PTFE baiting valve, Φ18mm baiting port, inclined discharging nozzle (Pagoda joint), Φ12mm,from floor 350mm |
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Vacuum suction nozzle |
24# glass suction nozzle(Pagoda joint),outer diameter 10mm |
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In and out circulation nozzle of condenser coil |
Pagoda joint,outer diameter 10mm |
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Overall dimension (W*L*H) |
330*350*1220mm |
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Net weight |
17.5kg |
|
Packing dimension |
1200*400*450mm,0.22m³ |
|
Packing weight |
32.5kg |
|
Model |
GR-1 |
GR-2 |
GR-3 |
GR-5 |
Glass Material |
GG-17 |
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Frame Material |
304 Stainless steel |
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Reaction bottle capacity |
1L |
2L |
3L |
5L |
Jacketed Capacity |
0.4L |
0.5L |
0.6L |
0.8L |
Flanged out of the oil circulation port |
Low feed high outlet |
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Reaction bottle cover port |
5 ports |
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Discharge port distance to ground |
30mm |
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Temp. range |
-80~250ºC |
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Vacuum |
0.098Mpa |
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Stirring speed |
0-800rpm |
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Stirring diameter |
8mm |
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Stirring power |
40W |
40W |
90W |
90W |
Voltage(V/Hz) |
220V/50Hz |
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Dimension(mm) |
350*345*1000 |
350*345*1000 |
350*410*1250 |
350*410*1250 |
Packing size(mm) |
1200*480*400 |
1200*480*400 |
1380*500*400 |
1380*500*400 |
Packing weight(KG) |
32 |
32 |
38 |
38kg |
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